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ChemicalBook CAS DataBase List 4-Bromo-2-methoxyphenylboronic acid

4-Bromo-2-methoxyphenylboronic acid synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: sulfuric acid; potassium iodide; sodium nitrite / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexanes / -80 °C / Inert atmosphere
2.2: -80 - 20 °C / Inert atmosphere
2.3: 20 °C / Inert atmosphere

References:

Lin, David W.;Masuda, Takeshi;Biskup, Moritz B.;Nelson, Jonathan D.;Baran, Phil S. [Journal of Organic Chemistry,2011,vol. 76,# 4,p. 1013 - 1030]