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4-bromo-2-tert-butyl-1-nitrobenzene synthesis

2synthesis methods
850012-44-1 Synthesis
4-bromo-2-tert-butylphenylamine

850012-44-1
79 suppliers
$42.00/100mg

4-bromo-2-tert-butyl-1-nitrobenzene

923547-56-2
5 suppliers
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Yield:923547-56-2 32%

Reaction Conditions:

with sulfuric acid;dihydrogen peroxide in water;acetic acid at 80; for 3 h;Inert atmosphere;

References:

Arisawa, Mieko;Kuwajima, Manabu;Yamaguchi, Masahiko [Tetrahedron Letters,2010,vol. 51,# 23,p. 3116 - 3118] Location in patent:supporting information; experimental part