4-BROMO-4',4''-DIMETHOXYTRITYL ALCOHOL synthesis
- Product Name:4-BROMO-4',4''-DIMETHOXYTRITYL ALCOHOL
- CAS Number:431039-52-0
- Molecular formula:C21H19BrO3
- Molecular Weight:399.28
Yield:431039-52-0 82%
Reaction Conditions:
Stage #1: 1-bromo-4-methoxy-benzenewith magnesium in tetrahydrofuran; for 1 h;Heating;
Stage #2: Ethyl 4-bromobenzoate in tetrahydrofuran;Further stages.;
References:
Hatano, Tsukasa;Kato, Takashi [Tetrahedron,2008,vol. 64,# 36,p. 8368 - 8380]
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