4'-BroMo-4-butoxy-biphenyl synthesis
4synthesis methods
- Product Name:4'-BroMo-4-butoxy-biphenyl
- CAS Number:63619-63-6
- Molecular formula:C16H17BrO
- Molecular Weight:305.21
Yield:63619-63-6 95%
Reaction Conditions:
Stage #1: 4-bromo-4'-hydroxybiphenylwith potassium hydroxide in tetrahydrofuran at 20; for 0.5 h;
Stage #2: 1-bromo-butane in tetrahydrofuran; for 6 h;Reflux;
References:
Sandhu, Sana;Kumar, Rahul;Singh, Prabhpreet;Kumar, Subodh [Journal of Materials Chemistry C,2016,vol. 4,# 15,p. 3209 - 3216] Location in patent:supporting information