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ChemicalBook CAS DataBase List 4-(BROMOMETHYL)CYCLOPENTENE

4-(BROMOMETHYL)CYCLOPENTENE synthesis

3synthesis methods
7686-77-3 Synthesis
3-Cyclopentene-1-carboxylic acid

7686-77-3
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4-(BROMOMETHYL)CYCLOPENTENE

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / diethyl ether / 3 h / 34 °C
2: pyridine; bromine; triphenylphosphine / dichloromethane / 13 h / -15 - 20 °C

References:

Kozhushkov, Sergei I.;Langer, Rainer;Yufit, Dmitrii S.;Howard, Judith A. K.;Schill, Heiko;Demus, Dietrich;Miyazawa, Kazutoshi;De Meijere, Armin [European Journal of Organic Chemistry,2004,# 2,p. 289 - 303]