4-(Bromomethyl)-N,N-dimethylbenzamide synthesis
- Product Name:4-(Bromomethyl)-N,N-dimethylbenzamide
- CAS Number:69449-20-3
- Molecular formula:C10H12BrNO
- Molecular Weight:242.11
52780-16-2
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124-40-3
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Yield:69449-20-3 43%
Reaction Conditions:
Stage #1: dimethyl aminewith triethylamine in tetrahydrofuran; for 0.166667 h;Schlenk technique;Inert atmosphere;
Stage #2: 4-bromomethylbenzoyl chloride in tetrahydrofuran at 20; for 16 h;Schlenk technique;Inert atmosphere;
References:
Buter, Jeffrey;Doze, Anna M.;Feringa, Ben L.;Mondal, Anirban;Visser, Paco [Chemical Communications,2021,vol. 57,# 61,p. 7529 - 7532] Location in patent:supporting information
14062-78-3
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6232-88-8
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874-60-2
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