4-(butan-2-ylamino)benzamide synthesis
1synthesis methods
- Product Name:4-(butan-2-ylamino)benzamide
- CAS Number:1019497-02-9
- Molecular formula:C11H16N2O
- Molecular Weight:192.26
Yield:1019497-02-9 68%
Reaction Conditions:
with bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)];N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine;lithium hexamethyldisilazane;sodium t-butanolate in 1,4-dioxane at 65; for 21 h;Inert atmosphere;chemoselective reaction;
References:
Tardiff, Bennett J.;McDonald, Robert;Ferguson, Michael J.;Stradiotto, Mark [Journal of Organic Chemistry,2012,vol. 77,# 2,p. 1056 - 1071] Location in patent:experimental part