4'-Butyl-4-biphenylcarbonitrile synthesis
- Product Name:4'-Butyl-4-biphenylcarbonitrile
- CAS Number:52709-83-8
- Molecular formula:C17H17N
- Molecular Weight:235.32
92-52-4
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$9.00/5g
52709-83-8
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$7.00/250mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: AlCl3 / CH2Cl2 / 5 h / Ambient temperature
2: 1) hydrazine hydrate, 2) KOH / 1) diethylene glycol, 130 deg C, 1 h, 2) diethylene glycol, 130 deg C, 2 h, then 160 deg C, 3 h
3: 1) TiCl4, 2) hydroxylamine hydrochloride, pyridine / 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h
4: 70 percent / acetic anhydride / 2 h / Heating
References:
Ruolene, Yu. I.;Adomenas, P. V.;Sirutkaitis, R. A.;Denis, G. I. [Journal of Organic Chemistry USSR (English Translation),1984,vol. 20,p. 1187 - 1191][Zhurnal Organicheskoi Khimii,1984,vol. 20,# 6,p. 1305 - 1310]
623-26-7
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$15.00/5G
109-65-9
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$10.00/10g
100-47-0
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$14.14/25gm:
1591-30-6
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$44.00/1g
104-51-8
166 suppliers
$14.00/1mL
52709-83-8
188 suppliers
$7.00/250mg
20651-73-4
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$45.00/100mg
![[1,1'-Biphenyl]-4-carboxaldehyde, 4'-butyl-, oxime](/CAS/20210305/GIF/93972-13-5.gif)
93972-13-5
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52709-83-8
188 suppliers
$7.00/250mg
37909-95-8
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$7.00/5g
52709-83-8
188 suppliers
$7.00/250mg
13211-01-3
135 suppliers
$29.00/25g
52709-83-8
188 suppliers
$7.00/250mg