4-CHLORO-2-PROPYL-PYRIDINE synthesis
- Product Name:4-CHLORO-2-PROPYL-PYRIDINE
- CAS Number:93856-98-5
- Molecular formula:C8H10ClN
- Molecular Weight:155.62
Yield:93856-98-5 83%
Reaction Conditions:
Stage #1: 4-chIoro-2-methylpyridinewith lithium diisopropyl amide in tetrahydrofuran at -78; for 0.5 h;
Stage #2: ethyl iodide in tetrahydrofuran at -78 - -30; for 1.5 h;
References:
Wiles, Jason A.;Hashimoto, Akihiro;Thanassi, Jane A.;Cheng, Jijun;Incarvito, Christopher D.;Deshpande, Milind;Pucci, Michael J.;Bradbury, Barton J. [Journal of Medicinal Chemistry,2006,vol. 49,# 1,p. 39 - 42]
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