4-CHLORO-2-TRIMETHYLSILYLPYRIDINE synthesis
- Product Name:4-CHLORO-2-TRIMETHYLSILYLPYRIDINE
- CAS Number:139585-50-5
- Molecular formula:C8H12ClNSi
- Molecular Weight:185.73
626-61-9
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$365.00/500mg
75-77-4
564 suppliers
$5.04/10
139585-50-5
25 suppliers
$45.00/50mg
Yield:139585-50-5 85%
Reaction Conditions:
Stage #1: 4-Chloropyridinewith n-butyllithium in hexane at -78; for 1 h;
Stage #2: chloro-trimethyl-silanewith hexachloroethane in tetrahydrofuran;hexane at -78 - 20; for 1 h;
References:
Choppin, Sabine;Gros, Philippe;Fort, Yves [European Journal of Organic Chemistry,2001,# 3,p. 603 - 606]
75-77-4
564 suppliers
$5.04/10
22918-01-0
259 suppliers
$6.00/1g
139585-50-5
25 suppliers
$45.00/50mg