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ChemicalBook CAS DataBase List 4-CHLORO-6-FLUOROINDAN-1-ONE

4-CHLORO-6-FLUOROINDAN-1-ONE synthesis

3synthesis methods
84194-36-5 Synthesis
2-Chloro-4-fluorobenzaldehyde

84194-36-5
339 suppliers
$9.00/1g

-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 96 percent / pyridine; piperidine / 18 h / 70 °C
2: 98 percent / H2 / platinum oxide / aq. ethanol
3: oxalyl chloride / CH2Cl2 / 20 °C
4: aluminum chloride / CH2Cl2 / 2.5 h / Heating

References:

Musso, David L.;Orr, G. Faye;Cochran, Felicia R.;Kelley, James L.;Selph, Jeffrey L.;Rigdon, Greg C.;Cooper, Barrett R.;Jones, Michael L. [Journal of Medicinal Chemistry,2003,vol. 46,# 3,p. 409 - 416]

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