4-CHLORO-6-(METHYLTHIO)PYRIMIDINE-5-CARBONITRILE synthesis

3synthesis methods

Product Name:4-CHLORO-6-(METHYLTHIO)PYRIMIDINE-5-CARBONITRILE
CAS Number:150807-96-8
Molecular formula:C6H4ClN3S
Molecular Weight:185.63

METHYL 2-CYANO-3,3-DI(METHYLTHIO)ACRYLATE

3490-92-4
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4-CHLORO-6-(METHYLTHIO)PYRIMIDINE-5-CARBONITRILE

150807-96-8
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: Et₃N / ethanol / 5 h / Heating
2: POCl₃ / 7 h / Heating

References:

Liu, Chunjian;Wrobleski, Stephen T.;Lin, James;Ahmed, Gulzar;Metzger, Axel;Wityak, John;Gillooly, Kathleen M.;Shuster, David J.;McIntyre, Kim W.;Pitt, Sidney;Shen, Ding Ren;Zhang, Rosemary F.;Zhang, Hongjian;Doweyko, Arthur M.;Diller, David;Henderson, Ian;Barrish, Joel C.;Dodd, John H.;Schieven, Gary L.;Leftheris, Katerina [Journal of Medicinal Chemistry,2005,vol. 48,# 20,p. 6261 - 6270]

4-(METHYLTHIO)-6-OXO-1,6-DIHYDROPYRIMIDINE-5-CARBONITRILE

16071-28-6
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150807-96-8
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References

17823-58-4 Synthesis

3,3-BIS(METHYLTHIO)-2-CYANOACRYLIC ACID ETHYL ESTER

17823-58-4
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$45.00/250mg

150807-96-8
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References

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4-CHLORO-5-CYANO-2-METHYL-6-(METHYLTHIO)PYRIMIDINE