4-CHLORO-N'-(2-CHLOROACETYL)BENZENECARBOHYDRAZIDE synthesis
- Product Name:4-CHLORO-N'-(2-CHLOROACETYL)BENZENECARBOHYDRAZIDE
- CAS Number:50677-27-5
- Molecular formula:C9H8Cl2N2O2
- Molecular Weight:247.08
Yield:50677-27-5 88%
Reaction Conditions:
Stage #1: chloroacetic acidwith 2,6-dimethylpyridine;O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate in dichloromethane at 25; for 0.166667 h;
Stage #2: 4-chlorobenzoic acid hydrazide at 20; for 3 h;
References:
Gurupadaswamy, Handuvinahalli Devanna;Girish, Virupaksha;Zameer, Farhan;Hegdekatte, Raghavendra;Chauhan, Jyoti Bala;Khanum, Shaukath Ara [Archiv der Pharmazie,2013,vol. 346,# 11,p. 805 - 811]
7335-27-5
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