4-CHLOROBENZENEDIAZONIUM HEXAFLUOROPHOSPHATE synthesis
- Product Name:4-CHLOROBENZENEDIAZONIUM HEXAFLUOROPHOSPHATE
- CAS Number:1582-27-0
- Molecular formula:C6H4ClF6N2P
- Molecular Weight:284.53
106-47-8
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Yield:1582-27-0 58%
Reaction Conditions:
Stage #1: 4-chloro-anilinewith hydrogen hexafluorophosphate (V) in water monomer at 20; for 0.0333333 h;Inert atmosphere;
Stage #2: with NaNO2 in water monomer at 0; for 0.25 h;Inert atmosphere;
References:
Akram, Manjur O.;Mali, Pramod S.;Patil, Nitin T. [Organic Letters,2017,vol. 19,# 12,p. 3075 - 3078] Location in patent:supporting information