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ChemicalBook CAS DataBase List 4-CYANO-3-(TRIFLUOROMETHYL)ACETANILIDE
97760-99-1

4-CYANO-3-(TRIFLUOROMETHYL)ACETANILIDE synthesis

4synthesis methods
-

Yield:928312-11-2 83%

Reaction Conditions:

Stage #1: C11H14O4;4-amino-2-trifluoromethylbenzonitrilewith dmap;thionyl chloride in tetrahydrofuran at 20; for 120 h;
Stage #2: acetic anhydridewith pyridine in tetrahydrofuran;Further stages.;

References:

Fujino, Aya;Asano, Masayoshi;Yamaguchi, Hitomi;Shirasaka, Naoki;Sakoda, Akiko;Ikunaka, Masaya;Obata, Rika;Nishiyama, Shigeru;Sugai, Takeshi [Tetrahedron Letters,2007,vol. 48,# 6,p. 979 - 983]

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