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(4-CYANO-PHENYL)-PHOSPHONIC ACID synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 95 percent Spectr. / K2CO3, BTEAC / Pd(OAc)2, tris(2-furyl)phosphine / acetonitrile / 21 h / 70 - 80 °C
2: HCl, H2O / 8 h / Heating

References:

Kabachnik;Solntseva;Izmer;Novikova;Beletskaya [Russian Journal of Organic Chemistry,1998,vol. 34,# 1,p. 93 - 97]

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