4-(diethoxyMethyl)pyriMidin-2-aMine synthesis
- Product Name:4-(diethoxyMethyl)pyriMidin-2-aMine
- CAS Number:1014-03-5
- Molecular formula:C9H15N3O2
- Molecular Weight:197.23
Yield:1014-03-5 95%
Reaction Conditions:
Stage #1: guanidine hydrochloridewith sodium hydride in ethanol at 20; for 0.25 h;Inert atmosphere;
Stage #2: 1,1-diethoxybut-3-yn-2-one in ethanol at 20; for 0.75 h;Inert atmosphere;
References:
Sengee, Myagmarsuren;Sydnes, Leiv K. [Synthesis,2011,# 23,art. no. Z78711SS,p. 3899 - 3907] Location in patent:experimental part
851900-14-6
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