4-(Dimethylamino)cinnamaldehyde synthesis
- Product Name:4-(Dimethylamino)cinnamaldehyde
- CAS Number:6203-18-5
- Molecular formula:C11H13NO
- Molecular Weight:175.23
3054-95-3
207 suppliers
$28.00/25g
586-77-6
433 suppliers
$5.00/10g
6203-18-5
274 suppliers
$6.00/250mg
Yield:6203-18-5 77%
Reaction Conditions:
Stage #1: acrylaldehyde diethyl acetal;4-bromo-N,N-dimethylanilinewith potassium chloride;tetrabutylammonium acetate;potassium carbonate in N,N-dimethyl acetamide at 120; for 2.5 h;Heck reaction;
Stage #2: with hydrogenchloride in water;ethyl acetate at 20;chemospecific reaction;
References:
Alacid, Emilio;Najera, Carmen [European Journal of Organic Chemistry,2008,# 18,p. 3102 - 3106] Location in patent:experimental part
![2-Propen-1-ol, 3-[4-(dimethylamino)phenyl]-](/CAS/20210111/GIF/20850-05-9.gif)
20850-05-9
0 suppliers
inquiry
6203-18-5
274 suppliers
$6.00/250mg
586-77-6
433 suppliers
$5.00/10g
927-63-9
204 suppliers
$14.00/1g
6203-18-5
274 suppliers
$6.00/250mg
586-77-6
433 suppliers
$5.00/10g
107-02-8
4 suppliers
$38.60/4s8501
6203-18-5
274 suppliers
$6.00/250mg
52509-14-5
228 suppliers
$5.00/5g
100-10-7
608 suppliers
$5.00/1g
6203-18-5
274 suppliers
$6.00/250mg