4-(Dimethylamino)cinnamaldehyde synthesis
- Product Name:4-(Dimethylamino)cinnamaldehyde
- CAS Number:6203-18-5
- Molecular formula:C11H13NO
- Molecular Weight:175.23
3054-95-3
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586-77-6
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6203-18-5
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Yield:6203-18-5 77%
Reaction Conditions:
Stage #1: acrylaldehyde diethyl acetal;4-bromo-N,N-dimethylanilinewith potassium chloride;tetrabutylammonium acetate;potassium carbonate in N,N-dimethyl acetamide at 120; for 2.5 h;Heck reaction;
Stage #2: with hydrogenchloride in water;ethyl acetate at 20;chemospecific reaction;
References:
Alacid, Emilio;Najera, Carmen [European Journal of Organic Chemistry,2008,# 18,p. 3102 - 3106] Location in patent:experimental part
![2-Propen-1-ol, 3-[4-(dimethylamino)phenyl]-](/CAS/20210111/GIF/20850-05-9.gif)
20850-05-9
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6203-18-5
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$6.00/250mg
586-77-6
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927-63-9
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6203-18-5
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$6.00/250mg
586-77-6
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107-02-8
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6203-18-5
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52509-14-5
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100-10-7
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6203-18-5
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$6.00/250mg