4'-dimethylaminoacetanilide synthesis
- Product Name:4'-dimethylaminoacetanilide
- CAS Number:7463-28-7
- Molecular formula:C10H14N2O
- Molecular Weight:178.23
Yield:7463-28-7 97%
Reaction Conditions:
with C15H29IrN4(2+)*2I(1-) at 120; for 17 h;Inert atmosphere;Schlenk technique;Sealed tube;
Steps:
N,N-Dimethylation of a Variety of Aromatic Amines with Methanol Catalyzed by 4a Shown in Scheme 2; General Procedure
General procedure: In a stainless reactor bomb, the respective aromatic amine (1.0mmol), 4a (2.0 mol%), and MeOH (1.0 mL) were placed. Then, the reactor was sealed with a stainless stopper, and the mixture was stirred for 17 h at 120 °C. After removing MeOH under reduced pressure, the products were isolated by silica gel column chromatography.
References:
Toyooka, Genki;Tuji, Akiko;Fujita, Ken-Ichi [Synthesis,2018,vol. 50,# 23,p. 4617 - 4626]
![Ethanone, 1-[4-(dimethylamino)phenyl]-, oxime, (1E)-](/CAS/20210305/GIF/187672-34-0.gif)
187672-34-0
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