4-[(ETHOXYCARBONYL)AMINO]BENZOIC ACID synthesis
10synthesis methods
- Product Name:4-[(ETHOXYCARBONYL)AMINO]BENZOIC ACID
- CAS Number:5180-75-6
- Molecular formula:C10H11NO4
- Molecular Weight:209.2
Yield:5180-75-6 98%
Reaction Conditions:
Stage #1: chloroformic acid ethyl ester;4-amino-benzoic acidwith TEA in tetrahydrofuran at 20; for 1 h;
Stage #2: with trifluoroacetic acid for 1 h;Heating;
References:
Chilin, Adriana;Marzaro, Giovanni;Zanatta, Samuele;Barbieri, Vera;Pastorini, Giovanni;Manzini, Paolo;Guiotto, Adriano [Tetrahedron,2006,vol. 62,# 52,p. 12351 - 12356]
