4-ETHOXYPHENETHYLAMINE synthesis
- Product Name:4-ETHOXYPHENETHYLAMINE
- CAS Number:56370-30-0
- Molecular formula:C10H15NO
- Molecular Weight:165.2322
![Phenol, 4-[2-[[(4-methylphenyl)methylene]amino]ethyl]-](/CAS/20210305/GIF/1085313-37-6.gif)
1085313-37-6
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Yield:56370-30-0 91.8%
Reaction Conditions:
Stage #1: 4-(2-(4-methylbenzylideneamino)ethyl)phenol;ethyl iodidewith caesium carbonate in tert-butyl methyl ether;N,N-dimethyl-formamide at 40 - 53; for 4 h;Inert atmosphere;
Stage #2: with hydrogenchloride in water;ethyl acetate at 25; for 4 h;
References:
Magnus, Nicholas A.;Astleford, Bret A.;Brennan, John;Stout, James R.;Tharp-Taylor, Roger W. [Organic Process Research and Development,2009,vol. 13,# 2,p. 280 - 284] Location in patent:experimental part