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23328-64-5

4-ethyl-2,6-dihydroxynicotinonitrile synthesis

1synthesis methods
4949-44-4 Synthesis
Ethyl propionylacetate

4949-44-4
263 suppliers
$5.00/1g

4-ethyl-2,6-dihydroxynicotinonitrile

23328-64-5
6 suppliers
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Yield:23328-64-5 41%

Reaction Conditions:

with potassium hydroxide in methanol at 65; for 2 h;

References:

Renck, Daiana;MacHado, Pablo;Souto, Andre A.;Rosado, Leonardo A.;Erig, Thais;Campos, Maria M.;Farias, Caroline B.;Roesler, Rafael;Timmers, Luis F. S. M.;De Souza, Osmar N.;Santos, Diogenes S.;Basso, Luiz A. [Journal of Medicinal Chemistry,2013,vol. 56,# 21,p. 8892 - 8902] Location in patent:supporting information