4-ETHYLPHENYLZINC IODIDE synthesis
1synthesis methods
- Product Name:4-ETHYLPHENYLZINC IODIDE
- CAS Number:312693-04-2
- Molecular formula:C8H9IZn
- Molecular Weight:297.45
Yield:15290-87-6 27 %Chromat.
Reaction Conditions:
with chloro(1,5-cyclooctadiene)rhodium(I) dimer;3-diphenylphosphino-2-(diphenylphosphino)methyl-2-methylpropyl acetate in tetramethylurea at 20; for 24 h;Inert atmosphere;Negishi coupling reaction;
References:
Ejiri, Syogo;Odo, Shunsuke;Takahashi, Hideki;Nishimura, Yugo;Gotoh, Kazuma;Nishihara, Yasushi;Takagi, Kentaro [Organic Letters,2010,vol. 12,# 8,p. 1692 - 1695] Location in patent:supporting information; experimental part