4-(Ethylthio)toluene synthesis
- Product Name:4-(Ethylthio)toluene
- CAS Number:622-63-9
- Molecular formula:C9H12S
- Molecular Weight:152.26
6378-07-0
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622-63-9
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Yield:622-63-9 100 % Spectr.
Reaction Conditions:
Stage #1: ethyl (p-tolyl)sulfoxidewith oxalyl dichloride in tetrahydrofuran at -78; for 1 h;
Stage #2: with isopropyl alcohol in tetrahydrofuran at -78; for 1 h;
Stage #3: with triethylamine in tetrahydrofuran at -78 - 20;Further stages.;
References:
Bhatia, Gurpreet S.;Graczyk, Piotr P. [Tetrahedron Letters,2004,vol. 45,# 27,p. 5193 - 5195]
624-31-7
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93-89-0
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622-63-9
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$60.00/100mg
624-31-7
429 suppliers
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75-08-1
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$16.19/25ml
622-63-9
18 suppliers
$60.00/100mg