4-FLUORO-3-METHYLBENZOYL CHLORIDE synthesis
- Product Name:4-FLUORO-3-METHYLBENZOYL CHLORIDE
- CAS Number:455-84-5
- Molecular formula:C8H6ClFO
- Molecular Weight:172.58
403-15-6
192 suppliers
$5.00/1g
455-84-5
102 suppliers
$15.00/1g
Yield: 100%
Reaction Conditions:
with thionyl chloride for 1 h;Heating / reflux;
Steps:
29.a
14.00 g (90.8 mmol) 4-fluoro-3-methyl-benzoic acid are refluxed for 1 hour together with 50 ml of thionyl chloride and then evaporated down i. vac. The residue is further reacted without any more purification. Yield: 15.70 g (quantitative) C8H6ClFO (172.59)
References:
Boehringer Ingelheim International GmbH US2005/203078, 2005, A1 Location in patent:Page/Page column 42
95-52-3
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$10.00/5 g
455-84-5
102 suppliers
$15.00/1g
369-32-4
180 suppliers
$10.00/1g
455-84-5
102 suppliers
$15.00/1g