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ChemicalBook CAS DataBase List 4-Fluoro-7-nitrobenzofurazan
29270-56-2

4-Fluoro-7-nitrobenzofurazan synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 23 °C / Inert atmosphere
2: sodium azide / dimethyl sulfoxide / 2.5 h / 23 °C / Inert atmosphere
3: sodium nitrate; sulfuric acid / water / 0.07 h / 0 °C / Inert atmosphere

References:

Jung, Michael E.;Dong, Timothy A.;Cai, Xiaolu [Tetrahedron Letters,2011,vol. 52,# 20,p. 2533 - 2535]

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