ChemicalBook CAS DataBase List 4-HYDRAZINO-BENZOIC ACID ETHYL ESTER HCL

4-HYDRAZINO-BENZOIC ACID ETHYL ESTER HCL synthesis

4synthesis methods

Product Name:4-HYDRAZINO-BENZOIC ACID ETHYL ESTER HCL
CAS Number:40566-85-6
Molecular formula:C9H13ClN2O2
Molecular Weight:216.67

5798-75-4 Synthesis

5798-75-4
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4-HYDRAZINO-BENZOIC ACID ETHYL ESTER HCL

40566-85-6
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Yield:40566-85-6 95%

Reaction Conditions:

Stage #1: Ethyl 4-bromobenzoatewith nickel(II) bromide trihydrate;(4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate;1,8-diazabicyclo[5.4.0]undec-7-ene in dimethyl sulfoxide at 120; for 0.166667 h;Irradiation;Flow reactor;
Stage #2: with hydrogenchloride in 1,4-dioxane at 20; for 4 h;Inert atmosphere;

References:

Mata, Alejandro;Tran, Duc N.;Weigl, Ulrich;Williams, Jason D.;Kappe, C. Oliver [Chemical Communications,2020,vol. 56,# 93,p. 14621 - 14624] Location in patent:supporting information

94-09-7 Synthesis

94-09-7
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40566-85-6
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References

1,2,3-Oxadiazolium, 3-[4-(ethoxycarbonyl)phenyl]-5-hydroxy-, inner salt

89101-11-1
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40566-85-6
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References

64-17-5 Synthesis

64-17-5
707 suppliers
$10.00/50g

619-67-0 Synthesis

619-67-0
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$6.00/5g

40566-85-6
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References