ChemicalBook CAS DataBase List 4-HYDROXY-6-METHOXYMETHYL-2-(METHYLTHIO)PYRIMIDINE

4-HYDROXY-6-METHOXYMETHYL-2-(METHYLTHIO)PYRIMIDINE synthesis

3synthesis methods

Product Name:4-HYDROXY-6-METHOXYMETHYL-2-(METHYLTHIO)PYRIMIDINE
CAS Number:68087-13-8
Molecular formula:C7H10N2O2S
Molecular Weight:186.23

4-HYDROXY-6-METHOXYMETHYL-2-(METHYLTHIO)PYRIMIDINE

68087-13-8
35 suppliers
$81.29/1gm:

(5-chloro-6-Methyl-2-(Methylthio)pyriMidin-4-yl)Methanol

1374134-63-0
6 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 4 steps
1: N-chloro-succinimide / dichloromethane; N,N-dimethyl-formamide / 4 h / 20 °C
2: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 20 °C
3: caesium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1 h / 140 °C
4: boron tribromide / dichloromethane / 1 h / 0 °C

References:

WO2012/58187,2012,A1

68087-13-8
35 suppliers
$81.29/1gm:

1374134-65-2
1 suppliers
inquiry

References

68087-13-8
35 suppliers
$81.29/1gm:

5-Chloro-6-(methoxymethyl)-2-(methylthio)-4-pyrimidinyl 1,1,1-trifluoromethanesulfonate

1374134-61-8
0 suppliers
inquiry

References