4-HYDROXY-7-IODOQUINOLINE synthesis

6synthesis methods

Product Name:4-HYDROXY-7-IODOQUINOLINE
CAS Number:22297-71-8
Molecular formula:C9H6INO
Molecular Weight:271.05

3-Quinolinecarboxylic acid, 4-hydroxy-7-iodo-

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Yield:22297-71-8 98%

Reaction Conditions:

at 280; for 15 h;

Steps:

6

Compound 6-E (5.5 g) was placed I a 100 mL round bottom flask and heated under N2 in an oil bath to 280 C for 15 minutes. 7-iodoquinolin-4-ol 6-F (4.6 g, 99% yield) was obtained as a solid.

References:

WO2005/63739,2005,A1 Location in patent:Page/Page column 53

ethyl 4-hydroxy-7-iodoquinoline-3-carboxylate

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References

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References

2-Quinolinecarboxylic acid, 4-hydroxy-7-iodo-

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References

626-01-7 Synthesis

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References