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4-IODO-1,2-BENZENEDIOL synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 1H-imidazole / tetrahydrofuran / 20 °C / Inert atmosphere
1.3: 20 °C
2.1: palladium(II) trimethylacetate; [bis(acetoxy)iodo]benzene / α,α,α-trifluorotoluene / 120 °C / Inert atmosphere
2.2: 20 °C

References:

Huang, Chunhui;Ghavtadze, Nugzar;Chattopadhyay, Buddhadeb;Gevorgyan, Vladimir [Journal of the American Chemical Society,2011,vol. 133,# 44,p. 17630 - 17633]