4-IODOTOLUENE-D7 synthesis
- Product Name:4-IODOTOLUENE-D7
- CAS Number:1039678-66-4
- Molecular formula:C7D7I
- Molecular Weight:225.08
106-49-0
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1039678-66-4
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$1525.00/0.5g
Yield:-
Reaction Conditions:
Stage #1: p-toluidinewith hydrogen;water-d2;palladium on activated charcoal;platinum on activated charcoal at 180; for 24 h;
Stage #2: with hydrogenchloride;sodium nitrite in water;acetone at 3 - 5; for 1.25 h;
Stage #3: with sodium iodide in water;acetone at -30 - 20; for 2.41667 h;Further stages.;
References:
Ito, Nobuhiro;Watahiki, Tsutomu;Maesawa, Tsuneaki;Maegawa, Tomohiro;Sajiki, Hironao [Synthesis,2008,# 9,art. no. F03608SS,p. 1467 - 1478]