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4-MEO-MIPT synthesis

2synthesis methods
4837-90-5 Synthesis
4-Methoxyindole

4837-90-5
308 suppliers
$14.00/1g

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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 95 percent / tert-butylcatechol / xylene / 3 h / Heating
2: H2 / 10 percent Pd/C / ethanol / 12 h / 2585.7 Torr
3: K2CO3 / H2O; toluene / 15 h / Ambient temperature
4: lithium aluminum hydride / tetrahydrofuran / 0.5 h / Heating
5: H2 / 10 percent Pd/C / ethanol / 15 h / 2585.7 Torr

References:

Repke, David B.;Grotjahn, Douglas B.;Shulgin, Alexander T. [Journal of Medicinal Chemistry,1985,vol. 28,# 7,p. 892 - 896]

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