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1092938-89-0

4-Methoxy-1-cyclohexenyl Trifluoromethanesulfonate synthesis

1synthesis methods
37595-74-7 Synthesis
N-Phenyl-bis(trifluoromethanesulfonimide)

37595-74-7
429 suppliers
$5.00/1g

13482-23-0 Synthesis
4-Methoxycyclohexanon

13482-23-0
200 suppliers
$20.00/250mg

4-Methoxy-1-cyclohexenyl Trifluoromethanesulfonate

1092938-89-0
1 suppliers
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Yield:1092938-89-0 78%

Reaction Conditions:

with lithium hexamethyldisilazane in tetrahydrofuran at -78 - 20; for 16 h;Inert atmosphere;

References:

Lou, Terry Shing-Bong;Bagley, Scott W.;Willis, Michael C. [Angewandte Chemie - International Edition,2019,vol. 58,# 52,p. 18859 - 18863][Angew. Chem.,2019,vol. 131,# 52,p. 19035 - 19039,5] Location in patent:supporting information