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4-Methoxy-but-2-ynoic acid synthesis

3synthesis methods
-

Yield:24303-64-8 94%

Reaction Conditions:

with 3-(1-mesityl-1H-imidazol-3-ium-3-yl)propane-1-sulfonate;caesium carbonate;potassium iodide;silver(l) oxide in N,N-dimethyl-formamide at 35; under 750.075 Torr; for 24 h;Darkness;

References:

Yuan, Ye;Chen, Cheng;Zeng, Cheng;Mousavi, Bibimaryam;Chaemchuen, Somboon;Verpoort, Francis [ChemCatChem,2017,vol. 9,# 5,p. 882 - 887]