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ChemicalBook CAS DataBase List (4-METHOXYBENZYL)PHOSPHONIC ACID

(4-METHOXYBENZYL)PHOSPHONIC ACID synthesis

2synthesis methods
-

Yield:40299-61-4 84.6%

Reaction Conditions:

Stage #1: bromobenzene;triethyl phosphite at 150; for 5.5 h;Inert atmosphere;Arbuzov Reaction;
Stage #2: with hydrogenchloride in water; for 24 h;Reflux;Inert atmosphere;

References:

Cai, Zhong-Sheng;Hoshino, Norihisa;Bao, Song-Song;Jia, Jiage;Akutagawa, Tomoyuki;Zheng, Li-Min [Chemistry - A European Journal,2018,vol. 24,# 51,p. 13495 - 13503]

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