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ChemicalBook CAS DataBase List (4-METHOXYCARBONYLMETHYLPHENYL)BORONIC ACID

(4-METHOXYCARBONYLMETHYLPHENYL)BORONIC ACID synthesis

4synthesis methods
14199-15-6 Synthesis
Methyl 4-hydroxyphenylacetate

14199-15-6
303 suppliers
$7.00/10g

-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: 98 percent / 2,6-lutidine / CH2Cl2 / -40 °C
2.1: 85 percent / potassium acetate; PdCl2(dppf) / dioxane / 80 °C
3.1: diethanolamine / propan-2-ol; diethyl ether
3.2: hydrochloric acid / H2O; tetrahydrofuran / 20 °C

References:

Wang, You-Chu;Georghiou, Paris E. [Organic Letters,2002,vol. 4,# 16,p. 2675 - 2678]

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