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86518-09-4

4-methoxyfuro[3,2-c]pyridine-2-carbaldehyde synthesis

1synthesis methods
31270-80-1 Synthesis
4-CHLOROFURO[3,2-C]PYRIDINE

31270-80-1
115 suppliers
$10.00/100mg

4-methoxyfuro[3,2-c]pyridine-2-carbaldehyde

86518-09-4
3 suppliers
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 59.6 percent / dimethylformamide / 1 h / Heating
2: 1.) t-butyl lithium / 1.) THF, -65 deg C, 5 min; -10 deg C, 15 min, 2.) -65 deg C to -60 deg C, 30 min; room temperature, 1 h

References:

Bisagni, E.;Hung, N. Chi;Lhoste, J. M. [Tetrahedron,1983,vol. 39,# 10,p. 1777 - 1782]