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15638-06-9

4-Methoxyphenanthrene synthesis

11synthesis methods
Benzenesulfonic acid, 4-methyl-, 1,1'-[2,2'-[(6-methoxy[1,1'-biphenyl]-2,2'-diyl)dimethylidyne]dihydrazide]

1392144-19-2
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4-Methoxyphenanthrene

15638-06-9
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Yield:15638-06-9 95%

Reaction Conditions:

with dirhodium tetraacetate;lithium tert-butoxide in toluene at 90; for 1 h;Inert atmosphere;Molecular sieve;

References:

Xia, Ying;Liu, Zhenxing;Xiao, Qing;Qu, Peiyuan;Ge, Rui;Zhang, Yan;Wang, Jianbo [Angewandte Chemie - International Edition,2012,vol. 51,# 23,p. 5714 - 5717] Location in patent:supporting information; experimental part