4-METHOXYPYRIDINE-2-CARBOXYLIC ACID synthesis
- Product Name:4-METHOXYPYRIDINE-2-CARBOXYLIC ACID
- CAS Number:29082-91-5
- Molecular formula:C7H7NO3
- Molecular Weight:153.14
1124-33-0
332 suppliers
$10.00/1g
29082-91-5
118 suppliers
$10.00/250mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: 2 h / 65 - 70 °C
2: 73 percent / H2O / -8 - -7 °C
3: 1.) 90percent H2SO4, 2.) NaNO2 / 1.) 120 deg C, 2 h, 2.) water, 20-25 deg C, 1 h, then 80 deg C, 1 h
4: 90 percent / Na / 2 h / Heating
References:
Desjardins, Sylvie Y.;Cavell, Kingsley J.;Hoare, Jason L.;Skelton, Brian W.;Sobolev, Alexander N.;White, Allan H.;Keim, Wilhelm [Journal of Organometallic Chemistry,1997,vol. 544,# 2,p. 163 - 174]
67-56-1
739 suppliers
$7.29/5ml-f
13509-19-8
148 suppliers
$30.00/250mg
29082-91-5
118 suppliers
$10.00/250mg
694-59-7
284 suppliers
$7.00/5g
29082-91-5
118 suppliers
$10.00/250mg
19235-88-2
124 suppliers
$9.00/100mg
29082-91-5
118 suppliers
$10.00/250mg