4-Methyl-2-phenylbenzo[b]thiophene synthesis
1synthesis methods
- Product Name:4-Methyl-2-phenylbenzo[b]thiophene
- CAS Number:162135-79-7
- Molecular formula:C15H12S
- Molecular Weight:224.32
Yield:162135-79-7 47%
Reaction Conditions:
with tert.-butylnitrite in nitromethane at 80; for 12 h;Schlenk technique;Inert atmosphere;
References:
Zang, Hao;Sun, Jian-Guo;Dong, Xin;Li, Ping;Zhang, Bo [Advanced Synthesis and Catalysis,2016,vol. 358,# 11,p. 1746 - 1752] Location in patent:supporting information