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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 4-METHYL-3-METHYLAMINOPYRIDINE

4-METHYL-3-METHYLAMINOPYRIDINE synthesis

6synthesis methods
593-51-1 Synthesis
Methylamine hydrochloride

593-51-1
531 suppliers
$21.00/100g

3430-22-6 Synthesis
3-Bromo-4-methylpyridine

3430-22-6
414 suppliers
$6.00/1g

4-METHYL-3-METHYLAMINOPYRIDINE

77862-24-9
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Yield: 87%

Reaction Conditions:

with copper;sodium hydroxide in water at 120 - 130; for 24 h;Autoclave;

Steps:

2 Preparation of compound III
Add compound II (100g, 0.58mol) and water (350g) into the autoclave,Add methylamine hydrochloride (196g, 2.90mol) and sodium hydroxide (120g, 3.0mol) sequentially.Add catalytic amount of copper powder under stirring. The temperature was slowly raised to 120-130°C, and the reaction was stirred for 24 hours.Cool to room temperature, extract three times with dichloromethane (500mL), dry,Concentrated to obtain compound III (61.6 g, yield 87%).

References:

CN112250615, 2021, A Location in patent:Paragraph 0046; 0060-0062

74-89-5 Synthesis
Methylamine

74-89-5
7 suppliers
$13.44/25ML

3430-22-6 Synthesis
3-Bromo-4-methylpyridine

3430-22-6
414 suppliers
$6.00/1g

4-METHYL-3-METHYLAMINOPYRIDINE

77862-24-9
48 suppliers
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References
3430-27-1 Synthesis
3-Amino-4-methylpyridine

3430-27-1
460 suppliers
$13.43/1gm:

124-41-4 Synthesis
Sodium Methoxide

124-41-4
683 suppliers
$12.00/25g

4-METHYL-3-METHYLAMINOPYRIDINE

77862-24-9
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References
3-CHLORO-4-METHYLPYRIDINE

72093-04-0
114 suppliers
$21.00/1g

74-89-5 Synthesis
Methylamine

74-89-5
7 suppliers
$13.44/25ML

4-METHYL-3-METHYLAMINOPYRIDINE

77862-24-9
48 suppliers
inquiry

References
694495-63-1 Synthesis
3-METHOXYCARBONYLAMINO-4-METHYLPYRIDINE

694495-63-1
66 suppliers
$59.00/100mg

4-METHYL-3-METHYLAMINOPYRIDINE

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References

4-METHYL-3-METHYLAMINOPYRIDINE Related Search:

Benzyl chloride Malonyl chloride N-((3R,4S)-1-benzyl-4-methylpiperidin-3-yl)-N-methyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine N-methyl-N-((3R,4R)-4-methylpiperidin-3-yl)-7H-pyrrolo[2,3-d]pyrimidin-4-amine 4-Chloro-7-tosyl-7H-pyrrolo[2,3-d]pyrimidine 4-(Hydroxyamino)-4-oxobutanoic acid N-Hydroxysuccinimide Pyrrolo[2,3-d]pyrimidin-4-ol 7H-Pyrrolo[2,3-d]pyrimidine-2,4-diol 7H-Pyrrolo[2,3-d]pyriMidin-4-aMine, N-Methyl-N-[(3R,4R)-4-Methyl-1-(phenylMethyl)-3-piperidinyl]-7-[(4-Met hylphenyl)sulfonyl]-