4-Methyloctanoic acid synthesis
- Product Name:4-Methyloctanoic acid
- CAS Number:54947-74-9
- Molecular formula:C9H18O2
- Molecular Weight:158.24
66-25-1
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54947-74-9
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: dimethylamine hydrochloride / H2O / 24 h / 70 °C
2: NaBH4; aq. NaHCO3 / methanol / 1 h / 5 °C
3: 76 percent / propionic acid / 5 h / 138 °C
4: H2 / Pd/C / ethanol / 3 h / 20 °C
5: 95 percent / aq. potassium hydroxide / ethanol / 2.5 h / Heating
References:
Ragoussis, Valentine;Giannikopoulos, Alexandros;Skoka, Efthymia;Grivas, Panagiotis [Journal of Agricultural and Food Chemistry,2007,vol. 55,# 13,p. 5050 - 5052]
56196-53-3
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50965-90-7
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1070-66-2
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