4-methylpentadecane synthesis
- Product Name:4-methylpentadecane
- CAS Number:2801-87-8
- Molecular formula:C16H34
- Molecular Weight:226.44
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Yield:-
Reaction Conditions:
with 0.30 wt % Pd loading SAPO-41 molecular sieve at 320; under 15001.5 Torr;Reagent/catalyst;Temperature;
Steps:
Catalytic Performance Tests
The hydroisomerization of n-hexadecane was carriedout in a fi xed-bed reactor with 1.0 g catalyst (20-40 mesh)over all catalysts. Before the test, the catalyst was placedinto the reaction tube and treated under a fl ow of H2 at400°C for 1 h. Furthermore, the tests were conducted atweight hourly space velocity (WHSV) of 3.70 h-1, H2pressure of 2.0 MPa, H2/n-hexadecane molar ratio of8.72 and reaction temperature at the range of 280-370°C.The reaction products were analyzed by using the Agilent6820 gas chromatograph, which was equipped witha fl ame ionization detector (FID) and a HP-1 capillarycolumn (60 m × 0.25 mm × 1.00 μm). The conversion ofn-hexadecane (%) and the yield of iso-hexadecane (%)are calculated by the following formula: Conversion of -hexadecane the amount of -hexadecane consumed 100,the amount of -hexadecane in feedn nn 100%, Selectivity to -hexadecane the amount of -hexadecane formed 100,amount of -hexadecane consumediso ison Yield of -hexadecane the amount of -hexadecane formed 100,the amount of -hexadecane in feediso ison 100%,100%,
References:
Bai, Xuefeng;Guo, Chunmu;Jia, Guozhi;Li, Tong;Maximov, A. L.;Su, Xiaofang;Wang, Wei;Wei, Xiaomeng;Wu, Wei [Russian Journal of Applied Chemistry,2020,vol. 93,# 4,p. 502 - 511][Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.),2020,# 4]
