4-(METHYLTHIO)-1-BUTYLAMINE synthesis
- Product Name:4-(METHYLTHIO)-1-BUTYLAMINE
- CAS Number:55021-77-7
- Molecular formula:C5H13NS
- Molecular Weight:119.23
52096-68-1
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55021-77-7
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Yield:55021-77-7 83.2%
Reaction Conditions:
with hydrazine monohydrate in ethanol; for 5 h;Reflux;
Steps:
2.3
(3) Intermediate 23.11 g (67.7%, 8.44 mmol) was dissolved in 50 ml of absolute ethanol, and 2 times the amount of hydrazine hydrate was slowly added dropwise. Heating and refluxing for 5h, cooling to 0 ° C, fully precipitating, filtering, washing with ether, the filtrate is combined and concentrated in vacuo to give 0.871g of colorless liquid. The intermediate content of GC-MS is about 96.1%. The yield of intermediate III was about 83.2%.
References:
CN106496086,2017,A Location in patent:Paragraph 0013; 0051; 0057; 0063
59121-24-3
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55021-77-7
42 suppliers
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27160-24-3
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55021-77-7
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57775-01-6
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55021-77-7
42 suppliers
$315.00/250mg