4-Nonyn-1-ol synthesis
- Product Name:4-Nonyn-1-ol
- CAS Number:49826-98-4
- Molecular formula:C9H16O
- Molecular Weight:140.22
5390-04-5
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: toluene-4-sulfonic acid / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere; Schlenk technique
2.2: 20 °C / Reflux; Inert atmosphere; Schlenk technique
2.3: 20 °C / Inert atmosphere; Schlenk technique
References:
Rawat, Vishal Kumar;Higashida, Kosuke;Sawamura, Masaya [Advanced Synthesis and Catalysis,2021,vol. 363,# 6,p. 1631 - 1637]
