![](/CAS/GIF/37062-63-8.gif)
4'-OCTYLOXYACETOPHENONE synthesis
- Product Name:4'-OCTYLOXYACETOPHENONE
- CAS Number:37062-63-8
- Molecular formula:C16H24O2
- Molecular Weight:248.36
![1-Bromooctane](/CAS/GIF/111-83-1.gif)
111-83-1
490 suppliers
$12.00/25g
![4'-Hydroxyacetophenone](/CAS/GIF/99-93-4.gif)
99-93-4
839 suppliers
$5.00/25g
![4'-OCTYLOXYACETOPHENONE](/CAS/GIF/37062-63-8.gif)
37062-63-8
19 suppliers
$712.00/1G
Yield:37062-63-8 99%
Reaction Conditions:
with potassium carbonate in N,N-dimethyl-formamide at 80; for 24 h;
Steps:
2 Synthesis of Compound 1
Take a clean two bottle, add magnet,1.36 g of p-hydroxyacetophenone (about 10 mmol),9.66 g of bromooctane (about 50 mmol),6.91 g of potassium carbonate and 40 ml of anhydrous N,N-dimethylformamide solution.Under magnetic stirring, react at 80°C for 24 h.After the reaction was completed, water/methylene chloride was extracted several times and the organic phases were combined.After separation by a chromatography column, 2.46 g of light yellow liquid was obtained (approximately 99% yield).
References:
CN107501313,2017,A Location in patent:Paragraph 0049; 0051; 0052
![N-OCTYL PHENYL ETHER](/CAS/GIF/1818-07-1.gif)
1818-07-1
61 suppliers
$182.00/10mL
![Acetyl chloride](/CAS/GIF/75-36-5.gif)
75-36-5
561 suppliers
$17.92/100G
![4'-OCTYLOXYACETOPHENONE](/CAS/GIF/37062-63-8.gif)
37062-63-8
19 suppliers
$712.00/1G
![N-OCTYL PHENYL ETHER](/CAS/GIF/1818-07-1.gif)
1818-07-1
61 suppliers
$182.00/10mL
![Acetic anhydride](/CAS/20180808/GIF/108-24-7.gif)
108-24-7
5 suppliers
$14.00/250ML
![4'-OCTYLOXYACETOPHENONE](/CAS/GIF/37062-63-8.gif)
37062-63-8
19 suppliers
$712.00/1G
![Phenol](/CAS/20180808/GIF/108-95-2.gif)
108-95-2
725 suppliers
$14.00/25g
![4'-OCTYLOXYACETOPHENONE](/CAS/GIF/37062-63-8.gif)
37062-63-8
19 suppliers
$712.00/1G