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4-octylphenylmethanethiol synthesis

6synthesis methods
67698-68-4 Synthesis
P-OCTYLOXYBENZYL ALCOHOL

67698-68-4
24 suppliers
$100.00/5g

Carbamimidothioic acid

17356-08-0
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4-octylphenylmethanethiol

869650-47-5
1 suppliers
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Yield:869650-47-5 77%

Reaction Conditions:

Stage #1: p-n-octyloxybenzyl alcohol;thioureawith toluene-4-sulfonic acid in acetonitrile; for 1 h;Heating;
Stage #2: with sodium hydroxide in acetonitrile; for 4 h;Heating;

References:

Hasegawa, Jun-Ya;Hamada, Masahiro;Miyamoto, Tetsuo;Nishide, Kiyoharu;Kajimoto, Tetsuya;Uenishi, Jun-Ichi;Node, Manabu [Carbohydrate Research,2005,vol. 340,# 15,p. 2360 - 2368]

110482-75-2 Synthesis
4-(Octyloxy)benzyl chloride

110482-75-2
12 suppliers
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4-octylphenylmethanethiol

869650-47-5
1 suppliers
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