4-PHENYLTHIOPHENOL synthesis
- Product Name:4-PHENYLTHIOPHENOL
- CAS Number:5633-55-6
- Molecular formula:C12H10OS
- Molecular Weight:202.27
Yield:5633-55-6 95%
Reaction Conditions:
with copper slag in N,N-dimethyl-formamide at 100; for 0.166667 h;Microwave irradiation;Green chemistry;Temperature;Wavelength;
Steps:
b. Microwave method.
General procedure: A round-bottom flask wascharged with a mixture of arylboronic acid 1a-1i(0.5 g), an equimolar amount of arenethiol 2a or 2b,and 20 mol % of copper slag in DMF (5 mL), and themixture was stirred for 10 min at 100°C under microwave irradiation (400 W). After completion of the reaction(TLC), the mixture was treated, and the product was isolated, as described above in a.
References:
Gavane, D. S.;Jambhorkar, V. S.;Kale, B. D.;Karnik, K. S.;Khandare, A. L.;Narula, I. S.;Rajhans, A. P.;Sarkate, A. P. [Russian Journal of Organic Chemistry,2020,vol. 56,# 7,p. 1300 - 1303]
14763-63-4
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