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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

4-Piperidinamine, 3,5-dimethyl- synthesis

2synthesis methods
3,5-Dimethyl-4-nitropyridine 1-oxide

14248-66-9
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4-Piperidinamine, 3,5-dimethyl-

100421-66-7
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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: PCl3 / CHCl3 / 1.5 h / 69.9 - 79.9 °C
2: 79.2 percent / LiAlH4 / diethyl ether / 2.5 h / Heating

References:

Puszynski, Andrzej;Rykowski, Zbigniew [Polish Journal of Chemistry,1984,vol. 58,# 7-8-9,p. 871 - 876]

3,5-Dimethyl-4-nitropyridine

89693-88-9
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4-Piperidinamine, 3,5-dimethyl-

100421-66-7
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References