4-Quinolinecarboxylic acid, 2-chloro-, ethyl ester synthesis
- Product Name:4-Quinolinecarboxylic acid, 2-chloro-, ethyl ester
- CAS Number:5467-61-8
- Molecular formula:C12H10ClNO2
- Molecular Weight:235.67
15733-89-8
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64-17-5
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5467-61-8
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Yield:5467-61-8 67%
Reaction Conditions:
Stage #1: 2-hydroxyquinoline-4-carboxylic acidwith trichlorophosphateInert atmosphere;Reflux;
Stage #2: with thionyl chloride for 2 h;Inert atmosphere;Reflux;
Stage #3: ethanolwith triethylamine for 0.5 h;Reflux;
References:
Kim, Hae Un;Sohn, Sunyoung;Choi, Wanuk;Kim, Minjun;Ryu, Seung Un;Park, Taiho;Jung, Sungjune;Bejoymohandas [Journal of Materials Chemistry C,2018,vol. 6,# 39,p. 10640 - 10658]
15733-89-8
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$14.14/1gm:
5467-61-8
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5467-57-2
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$6.00/250mg
5467-61-8
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91-56-5
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$5.00/25g
5467-61-8
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